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The proposed platform presented a well-defined voltammetric profile with a redox couple around 0. The proposed platform presented sensitivity, limit of detection, and limit of quantification of 0. The high importance of HZ in industrial, environmental and pharmaceutical fields have motivated the development of several analytical methodologies for HZ determination, such as spectrophotometry, 8 injection analysis based systems, 9 chromatographic methods, 10 , 11 and electrochemical methods. In this sense, the electrochemical methods show excellent performance for the determination of electroactive species in biological and environmental samples with good sensitivity, selectivity, low cost and high throughput. In addition, the electrochemical methods are portable, which facilitates the monitoring of molecules and the acquisition of information in situ and online.
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The proposed platform presented a well-defined voltammetric profile with a redox couple around 0. The proposed platform presented sensitivity, limit of detection, and limit of quantification of 0.

The high importance of HZ in industrial, environmental and pharmaceutical fields have motivated the development of several analytical methodologies for HZ determination, such as spectrophotometry, 8 injection analysis based systems, 9 chromatographic methods, 10 , 11 and electrochemical methods.

In this sense, the electrochemical methods show excellent performance for the determination of electroactive species in biological and environmental samples with good sensitivity, selectivity, low cost and high throughput.

In addition, the electrochemical methods are portable, which facilitates the monitoring of molecules and the acquisition of information in situ and online. A common strategy to detect HZ using electrochemical methods is the employment of chemically modified electrodes, which can improve the sensitivity and selectivity of the sensing device, improving the electrocatalytic activities for the electrochemical oxidation of HZ.

Co Salophen complex N,N’-bis salicylidene -1,2-phenylenediaminocobalt II was prepared according to methods previously published. The pH of the solutions was adjusted adding 0. Preparation of reduced graphene oxide rGO mg of the graphite oxide was dissolved in purified water and dispersed with the aid of a sonicator. Then, the pH of the solution was adjusted to 10 with ammonium hydroxide and The dispersion was left to cool and potassium chloride KCl was added to dispersion in order to favor the precipitation process by salting out effect.

Sensor construction A dispersion was prepared by mixing 3 mg of the reduced graphene oxide modified with Co Salophen complex with 1 mL of 2 mg mL-1 DNA dispersion. In order to modify the GCE with the composite, the surface of the GCE was polished with alumina slurry and, subsequently, it was copiously washed with water to remove any previously adsorbed material.

Preparation of the samples and electrochemical determination of HZ Drugs samples containing isoniazid INH from two different laboratories were purchased at local drugstores. The content of 5 capsules was macerated and The dispersion was filtered, transferred to a volumetric flask, and the volume was adjusted with water to mL. Results and Discussion Composite characterization The Fourier transformed infrared spectrum of rGO presented two peaks at and cm-1 corresponding to the stretching and bending vibration of OH groups of water molecules adsorbed on rGO Figure 1a.

As can be seen, the characteristic bands of compounds observed in spectra 1a and 1b were observed in spectrum 1c. Figure 2 shows CV obtained in the absence Figure 2 , curve d and presence Figure 2 , curve e of 0. Measurements were carried out in 0. In Figure 2 curve a , the anodic peak potential for oxidation of HZ at bare electrode occurs in an overpotential of between and mV, suggesting that the electron transfer between the surface of the bare electrode and the HZ is kinetically slow.

It was observed a significant increase of the anodic peak current of HZ with a shift of the anodic peak of HZ to about mV vs. Upon addition of 0. The plot of Ip vs. Date obtained from the Figure 3a:

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Скачать mp3 Total Security 10 2 0 Crack License Key Free Download. Total Security Premium 10 2 0 Crack Full Activation Key Cable Assembly Part Number Builder 41 2. Insulated Wire Today. Founded in , IW developed a unique PTFE . 1/2. 1/4. 1. 1 Optional protection for Outside Broadcast. However, many forms of graphene present low processability in a number of solvents as well as . The diffusion coefficient of HZ used was × cm2 s-1 .

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